High X-ray doses inhibit Ni4+/Ni3+ redox activity during delithiation in LiNiO2, with lower-dose regions showing normal behavior, allowing identification of a safe dose threshold for reliable operando measurements.
Beam damage in operando X-ray diffraction studies of Li-ion batteries
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Spatially inhomogeneous delithiation in LiNiO2 positive electrode: the effect of X-rays dose
High X-ray doses inhibit Ni4+/Ni3+ redox activity during delithiation in LiNiO2, with lower-dose regions showing normal behavior, allowing identification of a safe dose threshold for reliable operando measurements.