All four SEM Kikuchi diffraction geometries can reconstruct a full experimental diffraction sphere of aluminum, with transmission geometries preserving sharper higher-order details and reflection geometries limited by signal and distortion.
Advances in electron backscatter diffraction
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abstract
We present a few recent developments in the field of electron backscatter diffraction (EBSD). We highlight how open source algorithms and open data formats can be used to rapidly to develop microstructural insight of materials. We include use of AstroEBSD for single pixel based EBSD mapping and conventional orientation mapping; followed by an unsupervised machine learning approach using principal component analysis and multivariate statistics combined with a refined template matching method to rapidly index orientation data with high precision. Next, we compare a diffraction pattern captured using direct electron detector with a dynamical simulation and project this to create a high quality experimental "reference diffraction sphere". Finally, we classify phases using supervised machine learning with transfer learning and a convolutional neural network.
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cond-mat.mtrl-sci 1years
2024 1verdicts
CONDITIONAL 1representative citing papers
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Comparison of Kikuchi Diffraction Geometries in Scanning Electron Microscope
All four SEM Kikuchi diffraction geometries can reconstruct a full experimental diffraction sphere of aluminum, with transmission geometries preserving sharper higher-order details and reflection geometries limited by signal and distortion.