Activator solutions for geopolymers are most stable when used warm within about 1 to 1.5 minutes after mixing water, NaOH and sodium silicate in that order, and cooling can push them into an unstable, gelled state.
Comparison of embodied energies of Ordinary Portland Cement with Bayer-derived geopolymer products,
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Optimisation of Activator Solutions for Geopolymer Synthesis: Thermochemical Stability, Sequencing, and Standardisation
Activator solutions for geopolymers are most stable when used warm within about 1 to 1.5 minutes after mixing water, NaOH and sodium silicate in that order, and cooling can push them into an unstable, gelled state.