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Ultrafast synthesis of Pb-doped BiCuSeO oxyselenides by high-energy ball milling

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arxiv 1911.04843 v2 pith:CNXGPHAD submitted 2019-11-12 cond-mat.mtrl-sci

classification cond-mat.mtrl-sci
keywords bicuseomillingsynthesisballhigh-energyoxyselenidespb-dopedphase
verification ladder T0 review T1 audit T2 compute T3 formal
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We report on the direct ultrafast synthesis of Pb-doped BiCuSeO oxyselenides by high-energy ball milling. We show that, contrary to the mechanical alloying sintering routes used in the previous reports which require 7 - 13 hours to fabricate the BiCuSeO phase in powder form, this synthesis technique enables us to obtain pure phase materials at room temperature under air with milling time less than 60 minutes.

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