Nanoparticle manipulation with a carbon fiber tip in an electron microscope for μ-SQUID magnetometry

We report a carbon-fiber-tip based nanomanipulation system integrated into a scanning electron microscope for individual nanoparticle (NP) manipulation on a surface. Electrochemically etched amorphous carbon fiber tips with excellent mechanical rigidity and sub-100 nm apex radii effectively reduce the van der Waals adhesion and enable reliable positioning of about 100 nm size NPs with about 100 nm precision. This system combines a piezoelectric bimorph for vertical tip motion, a four-quadrant piezo-tube for two-dimensional fine tip control and a two-dimensional piezoelectric walker for coarse lateral translation. Using this setup, we successfully position single Fe$_3$O$_4$ magnetic NPs on micron sized superconducting quantum interference devices for optimal magnetic coupling between them and probe a NP's magnetism.