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Oblique diffraction geometry for the observation of several non-coplanar Bragg reflections under identical illumination

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arxiv 2504.08566 v1 pith:UX77AZGQ submitted 2025-04-11 cond-mat.mtrl-sci physics.optics

classification cond-mat.mtrl-sciphysics.optics
keywords latticediffractionreflectionsbragggeometrynon-coplanarobliquerotation
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We present a method to determine the strain tensor and local lattice rotation with Dark Field X-ray Microscopy. Using a set of at least 3 non-coplanar, symmetry-equivalent Bragg reflections, the illuminated volume of the sample can be kept constant for all reflections, facilitating easy registration of the measured lattice variations. This requires an oblique diffraction geometry, i.e.~the diffraction plane is neither horizontal nor vertical. We derive a closed, analytical expression that allows determination of the strain and lattice rotation from the deviation of experimental observables (e.g.~goniometer angles) from their nominal position for an unstrained lattice.

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  1. Bridging Grain Mapping and Dark Field X-ray Microscopy for Multiscale Diffraction Imaging

    physics.app-ph 2025-08 unverdicted novelty 6.0 of 10

    A transferable open-source workflow links grain mapping and dark-field X-ray microscopy, enabling targeted, non-destructive imaging from millimeter polycrystal structure to dislocations in iron.

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