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REVIEW 4 major objections 4 minor 155 references

Automating the analysis of micron-scale synchrotron diffraction data on inhomogeneous polycrystalline samples: a solid oxide electrolysis cell case study

T0 review · 4 major / 4 minor · reviewed 2026-08-03 · deepseek-v4-flash

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Pith's one-line read A fully automated software routine can turn micron-scale X-ray diffraction maps of layered electrochemical devices into per-pixel phase, lattice-parameter, and strain information, without any manual fitting or prior knowledge of the device

desk verdict Useful automation for 2D µ-XRD maps, honestly presented, but 'no prior architecture' is an overclaim and the pipeline needs benchmark validation before I'd trust the maps. read the letter →

arxiv 2607.28859 v1 pith:ND3O44PK submitted 2026-07-30 cond-mat.mtrl-sci cond-mat.otherphysics.acc-ph

Liam A. V. Nagle-Cocco , Christopher A. Crain , Michael J. Dzara , Mathias A. Kiefer , Madeline G. Port , Tolga Han Ulucan , Madeline Van Winkle , Oscar Hathaway
show 1 more author
Nicholas A. Strange
This is my paper · ORCID
classification cond-mat.mtrl-scicond-mat.otherphysics.acc-ph
keywords µ-XRDspatiallyresolveddiffractionRietveldrefinementPawleysolidoxideelectrolysercellautomatedphaseidentificationlatticeparameterspost-mortemcharacterization
verification ladder T0 review T1 audit T2 compute T3 formal

The pith

A machine-rendered reading of the paper's core claim, the machinery that carries it, and where it could break.

The reading

The paper sets out to remove the main bottleneck in micro-X-ray diffraction (µ-XRD) of inhomogeneous devices: a single 100 µm × 100 µm map can contain roughly 10,000 diffraction patterns, each with a different mix of phases, and conventional Rietveld analysis requires a person to know which phases are present and where. The authors propose an automated routine that tests a user-supplied list of candidate phases on every pattern, using peak matching and thresholds on goodness-of-fit, scale factor, and Pawley peak intensities, then refines the surviving phases together. They demonstrate it on a cross-section of a solid oxide electrolyser cell, recovering the positions of the air and fuel electrodes without being told them, mapping lattice-parameter gradients, and detecting reaction products such as SrO and NiO. If the approach works as claimed, spatially resolved, multi-phase crystallographic mapping becomes a routine post-mortem tool for electrolysers, batteries, and photovoltaic devices rather than a specialized manual effort.

What carries the argument

The load-bearing mechanism is a per-pattern phase-assignment decision tree wrapped around a Rietveld/Pawley refinement engine. A phase is kept only if characteristic peaks are present, the fit improves beyond a threshold, and the scale factor (or Pawley peak intensity, for coarse silver) exceeds a threshold. Because decisions are local, the routine never assumes where a phase should appear; it finds degradation products at unexpected positions and recovers layer boundaries from the data itself. Rietveld refinement fits a full crystal-structure model to the whole measured profile; Pawley refinement fits peak intensities without a full model.

What would settle it

Run the protocol on a cross-section whose true phase map is known independently (e.g., from electron microscopy), once with a real phase deliberately removed from the candidate list and once with a phase present at an abundance near the scale-factor threshold; if the pipeline returns a phase map that silently omits or misassigns those phases, the claim of complete automation is falsified.

Watch

Extended reading notes

Core claim

Central claim: phase identification and Rietveld refinement can be fully automated on two-dimensional µ-XRD datasets. For each pattern, the routine tests a user-supplied candidate phase list via characteristic-peak checks, Rietveld-fit comparisons with and without each phase, and thresholds on goodness-of-fit improvement, scale factor, and Pawley peak intensities; accepted phases are refined together, yielding spatial maps of phase presence, lattice parameters, scale factors, and fit quality. In the solid oxide electrolyser case study, it located the electrodes without architectural priors, reproduced a known lattice-parameter gradient near the air electrode, and mapped SrO, Ni, and NiO. The

Load-bearing premise

The load-bearing premise—conceded in the paper's own Conclusion—is that the user's candidate phase list is complete and that the fixed thresholds for peak matching, goodness-of-fit improvement, scale factor, and Pawley peak intensity remain valid at every position; if a real phase is absent from the list or falls just below a threshold, the automated assignment silently misses it.

Editorial extensions

If this is right

  • A 100 × 100 grid of µ-XRD patterns (10^4 patterns) can be reduced to per-pixel phase, lattice-parameter, scale-factor, and fit-quality maps with no pattern-by-pattern manual intervention.
  • Post-mortem degradation studies of solid oxide cells can map trace secondary phases (SrO, NiO, spinels), strain gradients, and oxygen-vacancy-related lattice-parameter changes that bulk diffraction averages away.
  • The measured reduction in GDC and LSCF unit-cell volume near the air electrode provides a spatially resolved proxy for oxygen-vacancy depletion, directly relevant to electrode performance.
  • Fit-quality maps act as physical diagnostics: poor fits clustered in the fuel electrode, traced to coarse-grained 8YSZ, reveal microstructural coarsening rather than an analysis failure.

Reading between the lines

Editorial extensions of the paper, not claims the author makes directly.

  • Beyond the paper, the fixed user-set thresholds could be calibrated from the dataset's own statistics—for example, the per-phase distribution of scale factors across all pixels—which would directly address the arbitrariness the authors concede in the Conclusion.
  • Beyond the paper, the near-identity of SrO and 8YSZ in symmetry and lattice parameter means the protocol's unique-assignment claim could be tested by rerunning the fuel-electrode data with 8YSZ removed from the candidate list; the paper itself raises this ambiguity for some SrO assignments.
  • Beyond the paper, treating goodness-of-fit as an output rather than an error flag suggests an automatic quality-control layer: pixels where fit quality correlates strongly with one phase's scale factor could be flagged for microstructural inspection, as the 8YSZ case demonstrates.
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Editorial analysis

A structured set of objections, weighed in public.

Desk editor's note, referee report, and a circularity audit.

Referee Report

4 major / 4 minor

Summary. The paper presents an automated analysis workflow for micron-focused synchrotron X-ray diffraction maps of chemically inhomogeneous polycrystalline samples. The protocol, built from Python scripts that drive Topas 7, performs phase identification through a sequence of peak-matching, Rietveld goodness-of-fit improvement, scale-factor, and Pawley intensity checks, then executes automated Rietveld/Pawley refinement over every pixel of a 2D map. The method is demonstrated on a solid oxide electrolysis cell cross-section, producing per-pixel phase-assignment maps and cubic lattice-parameter heatmaps for GDC, LSCF-6428, and 8YSZ, together with goodness-of-fit diagnostics and phase-scale-factor maps. The authors report a systematic decrease in lattice parameter near the air electrode, consistent with a prior µ-XRD linescan study by Nozaki et al. (2020), and interpret a high goodness-of-fit region in the fuel electrode as due to 8YSZ grain coarsening.

Significance. If the central claim—fully automated phase identification and Rietveld analysis of thousand-pixel µ-XRD datasets without manual intervention—is substantiated, the workflow would remove a major bottleneck in spatially resolved diffraction studies of energy devices. The open-source Python code with available data and the demanding multi-phase SOEC case study are concrete strengths, and the physical trend for GDC/LSCF lattice parameters is independently plausible and compared with earlier work. However, the claim of operation 'without prior knowledge of local architecture' is contradicted by the algorithm's own phase-co-occurrence rules, and the absence of uncertainty estimates and threshold-sensitivity analysis weakens the quantitative conclusions. The paper is a useful methods contribution, but it needs revision to align its claims with the actual inputs and to document reliability.

major comments (4)
  1. [§2 (Analysis protocol)] The phase-checking rules state that 'SrO, Fe/Co rocksalt, and Fe/Co spinel are only checked for at positions where LSCF-6428 is present, and Ni and NiO are only checked for if 8YSZ is present.' This is an explicit spatial/architectural prior: it encodes the layered arrangement of the SOEC and the expected co-occurrence of phases. It directly contradicts the abstract and §4 claim that the protocol works 'without prior knowledge of local architecture.' A phase appearing outside its expected co-occurrence context—for example, SrO after cation migration into the fuel electrode—would never be tested and would be silently missed. Since phase identification is the foundation of all downstream Rietveld maps, this overstatement is load-bearing and needs to be either removed from the claims or the algorithm modified to test all phases at all pixels (with associated computational cost acknowledged)
  2. [§2 and §4 (thresholds)] The phase-inclusion criteria rely on unstated thresholds for peak matching, goodness-of-fit improvement, scale factor, and Pawley peak intensities. The Conclusion concedes that the thresholds must be 'arbitrarily define[d]' and that the user must pre-specify the candidate phase list. No threshold values are given in the manuscript, and no sensitivity analysis is performed. The case study therefore does not demonstrate that the protocol is robust to reasonable variation in these thresholds across positions or chemistries. This is a load-bearing issue for the 'fully-automated' claim: the method is semi-automated with user-defined acceptance criteria. Please provide the actual threshold values used, and either show how the output maps change with threshold variation or explicitly frame the thresholds as a user-calibration step.
  3. [§4, Figure 4] The lattice-parameter heatmaps for GDC, LSCF-6428, and 8YSZ are presented without any uncertainty estimates. Rietveld refinement provides standard uncertainties that should be propagated onto the heatmaps (as error bars, color-scale uncertainties, or a separate uncertainty map). Without these, the claimed 'systematic variations' near the electrode surface cannot be distinguished from statistical noise, and the comparison with Nozaki et al. (2020) remains qualitative. Adding this would substantially strengthen the validation.
  4. [§3/§5, Figure 5 and Figure S5] Two issues affect the reliability of the reported lattice parameters. First, Figure 5 shows that the 8YSZ peakshape is poorly modelled in the fuel electrode, yet the protocol's 8YSZ lattice parameters and scale factors in those pixels are used in the analysis without flagging them as unreliable or quantifying the bias introduced by the misfit. Second, §2.1 and SI Figure S5 show that free refinement of zero error produced correlations with lattice parameters, so zero error was fixed to 0.01°. Fixing an instrumental parameter to a constant value across the map is a strong assumption, particularly given the authors' own note that beam path length may vary with surface roughness. The authors should justify the 0.01° value and assess the systematic error this induces in the lattice-parameter trends; at minimum, pixels with high goodness-of-fit should be identified as degraded in the maps.
minor comments (4)
  1. [Abstract] Grammar: '2D datasets of diffraction pattern taken' should be '2D datasets of diffraction patterns taken'.
  2. [§2] Sentence is garbled: 'For most phases, the assignment algorithm consists of (1), followed by (2) and (3) if algorithm (1) affirms the possible presence of the spinel phases.' This appears to reference only spinel phases but should describe the general rule. Please rewrite for clarity.
  3. [§3, last paragraph] Typo: 'damaged reasons should be removed' should read 'damaged regions should be removed'.
  4. [§5.3] Grammar/phrasing: 'This step size for the spatially-resolved measurements were...' should be 'The step size for the spatially-resolved measurements was...'. Also add scale bars to Figure 3(c) and the optical images in SI for quantitative interpretation.

Circularity Check

0 steps flagged · score 2.0 of 10

No circular derivation: empirical fitting pipeline with external benchmarks; architecture-dependent phase checks are a scope limitation, not a circular step.

full rationale

This paper presents an empirical analysis workflow, not a derivation, so the main circularity patterns (self-definitional equations, fitted parameters renamed as predictions, uniqueness theorems imported from the authors) do not apply. Phase models come from independent ICSD/external references (Table 1), and the Rietveld/Pawley machinery is standard Topas methodology. The central lattice-parameter/oxygen-vacancy trend is benchmarked against the independent prior µ-XRD study of Nozaki et al. (2020), and the 8YSZ peakshape explanation is tested in an independent powder experiment (Figure S14). Self-citations (Kaufman et al. 2026 in preparation; Crain et al. 2026; Zhu et al. 2026) are contextual or shared with independent support (Tyunina et al., 2021), so no load-bearing argument reduces to a self-citation. The closest issue is the paper's overclaim of operating 'without prior knowledge of local architecture': §2 states that 'SrO, Fe/Co rocksalt, and Fe/Co spinel are only checked for at positions where LSCF-6428 is present, and Ni and NiO are only checked for if 8YSZ is present,' which encodes phase co-occurrence—and for this layered SOEC, effectively architecture—into the search rules. The Conclusion also concedes 'the need to arbitrarily define threshold scale factors and goodness-of-fit improvements for phase assignments, and further to define the phases that might possibly occur in a dataset before beginning the analysis,' and the paper notes that near-fuel-electrode SrO assignments 'may in practice reflect cubic 8YSZ which is near-identical to SrO by diffraction.' These are genuine limitations on the autonomy claim, but they do not make any output equivalent to an input by construction: candidate phases must still pass peak-matching, goodness-of-fit, scale-factor, and intensity thresholds against measured diffraction data, and the major phase maps defining electrode positions are data-driven. The validation is partly a self-consistency check on a known SOEC architecture, which weakens the generality claim but does not constitute circular derivation of the reported phase, lattice-parameter, or strain-like results.

Assumptions & free parameters 2 free parameters · 3 assumptions · 0 invented entities

The scientific claims depend on user-set phase lists and thresholds, a fixed zero error, and standard powder-diffraction modeling assumptions; these are the hand-set inputs not purchased from prior literature.

free parameters (2)
  • Phase-inclusion thresholds (scale-factor, goodness-of-fit improvement, Pawley peak-intensity) = not reported
    The phase-assignment algorithm in Fig. 2 uses these cut-offs, but the paper never gives their values or a sensitivity analysis; the assignments (and hence phase maps) depend on them.
  • Fixed zero error = 0.01°
    After free refinement of zero error caused lattice-parameter correlations (SI Fig. S5), the zero error was fixed to 0.01° for all pixels; position-dependent sample height would invalidate this.
assumptions (3)
  • domain assumption The user-supplied candidate phase list is complete for the sample.
    The protocol can only assign phases from this list; unexpected degradation products or impurities would be missed. The Conclusion requires users to define the possible phases before analysis.
  • domain assumption Every Rietveld phase behaves as a fine powder, with intensities and peak shapes modeled by the TCH pseudo-Voigt function.
    The paper shows this fails for coarse-grained 8YSZ (Fig. 5c) and for Ag, which is given a Pawley treatment; if other phases violate it, lattice parameters may be biased.
  • domain assumption A single fixed zero error applies across the entire map.
    Fixed 0.01° assumes constant sample height/path length; the authors acknowledge surface texture could cause position-dependent zero error and hence biased lattice parameters.

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Cite this review

Pith. "Pith review of Automating the analysis of micron-scale synchrotron diffraction data on inhomogeneous polycrystalline samples: a solid oxide electrolysis cell case study." pith.science (2026). https://pith.science/paper/ND3O44PK

@misc{pith2026260728859,
  author       = {Pith},
  title        = {Pith review of: Automating the analysis of micron-scale synchrotron diffraction data on inhomogeneous polycrystalline samples: a solid oxide electrolysis cell case study},
  year         = {2026},
  howpublished = {\url{https://pith.science/paper/ND3O44PK}},
  note         = {Machine review of arXiv:2607.28859}
}
abstract

A novel approach to post mortem characterisation of electrochemical and photovoltaic devices is spatially-resolved diffraction using a hyper-focused, micron-width x-ray beam to examine the distribution of degradation products and strain, a technique called $\mu$-XRD. Aside from the experimental difficulties associated with beam focusing and sample preparation, which are themselves non-trivial, the analysis of resulting data is complex and challenging, with full Rietveld analysis rarely attempted in literature. The difficulty lies in the size of the data, which may consist of hundreds or even thousands of diffraction patterns with very different crystallographic phase compositions depending on position within the device, and the difficulty in fitting the data due to the presence of many phases at the same position, including possible degradation products which may be difficult to index and assign to known phases. In this paper, we present a fully-automated open access Python routine for performing phase identification and Rietveld analysis on 2D datasets of diffraction pattern taken at micron-scale positions, measured over the cross-section of a chemically inhomogeneous device with polycrystalline phases. Solid oxide electrolyser cells are a promising technology for green hydrogen production which can utilise waste heat to split water at higher efficiencies than low-temperature electrolysis techniques such as polymer electrolyte membranes, but exhibit many degradation modes due to the high operating temperatures. We present a case study using our analysis protocol on an SOEC fragment encompassing the air electrode, cation diffusion barrier, electrolyte, and fuel electrode. With modification, this protocol could be applied to other devices such as all-solid-state batteries, wet-electrolyte battery electrodes, solid oxide fuel cells, photovoltaic devices, and metal-oxide pseudocapacitors.

Figures

Figures reproduced from arXiv: 2607.28859 by the authors.

Figure 1
Figure 1. (a) Schematic illustrating the composition and design of the SOECs in this study. (b) [PITH_FULL_IMAGE:figures/full_fig_p003_1.png] view at source ↗
Figure 2
Figure 2. Schematic explaining, in partial pseudo-code, the approximate phase identification [PITH_FULL_IMAGE:figures/full_fig_p005_2.png] view at source ↗
Figure 3
Figure 3. (a) and (b) SEM images of a tombstone SOEC fragment from the same cell as the [PITH_FULL_IMAGE:figures/full_fig_p008_3.png] view at source ↗
Figures from the paper (2 more)
Figure 4
Figure 4. Figure 4: Heatmap visualising the lattice parameters of (a) GDC, (b) LSCF-6428, and (c) 8YSZ [PITH_FULL_IMAGE:figures/full_fig_p009_4.png]
Figure 5
Figure 5. Figure 5: (a) Heatmap showing the goodness-of-fit of fits across the SOEC. (b) Correlation plots [PITH_FULL_IMAGE:figures/full_fig_p010_5.png]

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Works this paper leans on

155 extracted references · 45 canonical work pages

  1. [1]

    AIP Conference Proceedings , volume=

    Full-Automatic XAFS Measurement System of the Engineering Science Research II beamline BL14B2 at SPring-8 , author=. AIP Conference Proceedings , volume=. 2010 , organization=

    2010

  2. [2]

    In preparation , year=

    GDC/YSZ diffraction study (in preparation) , author=. In preparation , year=

  3. [3]

    Cation Distributions and Anion Disorder in Ba _3 NbMO _

    Auckett, Josie E and Milton, Katherine L and Evans, Ivana Radosavljevic , journal=. Cation Distributions and Anion Disorder in Ba _3 NbMO _. 2019 , publisher=

    2019

  4. [4]

    Interlayer Ions Control Spin Canting in Low-Dimensional Manganese Trimers in 12R-Ba _4M Mn _3 O _

    Regier, Corlyn E and O’Donnell, Shaun and Goyal, Anuj and Dzara, Michael J and Park, James Eujin and Bell, Robert T and Kramer, Morgan J and Paddison, Joseph A M and Shulda, Sarah and Ginley, David S and Danielle R Yahne and Stephan Lany and Rebecca W Smaha and Ryan A Klein , journal=. Interlayer Ions Control Spin Canting in Low-Dimensional Manganese Trim...

    2024

  5. [5]

    H. T. Stokes and D. M. Hatch and B. J. Campbell , title =

  6. [6]

    2006 , publisher=

    Campbell, Branton J and Stokes, Harold T and Tanner, David E and Hatch, Dorian M , journal=. 2006 , publisher=

    2006

  7. [7]

    Magnetic characterization of layered Ba _6 Mn _5 O _

    Boulahya, K and Parras, M and Gonz. Magnetic characterization of layered Ba _6 Mn _5 O _. Physical Review B , volume=. 2004 , publisher=

    2004

  8. [8]

    Magnetic structure determination and refinement using

    Rodriguez-Carvajal, Juan and Gonzalez-Platas, Javier and Katcho, Nebil A , journal=. Magnetic structure determination and refinement using. 2025 , publisher=

    2025

Show all 155 references
  1. [9]

    Crystal and magnetic structures of Ba _4 Mn _3 O _

    Zubkov, V G and Tyutyunnik, A P and Berger, I F and Voronin, V I and Bazuev, G V and Moore, C A and Battle, P D , journal=. Crystal and magnetic structures of Ba _4 Mn _3 O _. 2002 , publisher=

    2002

  2. [10]

    Adkin, Josephine J and Hayward, Michael A , journal=. BaMnO _. 2007 , publisher=

    2007

  3. [11]

    Chemistry of Materials , volume=

    Crystal and magnetic structures of 2H BaMnO _3 , author=. Chemistry of Materials , volume=. 2000 , publisher=

    2000

  4. [12]

    Physica B: Condensed Matter , volume=

    The wide angle neutron diffractometer squared (WAND2)-possibilities and future , author=. Physica B: Condensed Matter , volume=. 2018 , publisher=

    2018

  5. [13]

    Naturwissenschaften , volume=

    Die gesetze der krystallochemie , author=. Naturwissenschaften , volume=. 1926 , publisher=

    1926

  6. [14]

    Green hydrogen production through low temperature thermochemical water splitting cycles based on non-ordered and ordered macroscopic structures of La0. 6Sr0. 4Co0. 2Fe0. 8O3 perovskite , author=. International Journal of Hydrogen Energy , volume=. 2025 , publisher=

    2025

  7. [15]

    Physica Scripta , volume=

    The Rietveld method , author=. Physica Scripta , volume=. 2014 , publisher=

    2014

  8. [16]

    Journal of Applied Crystallography , volume=

    Remote and automated high-throughput powder diffraction measurements enabled by a robotic sample changer at SSRL beamline 2-1 , author=. Journal of Applied Crystallography , volume=. 2023 , publisher=

    2023

  9. [17]

    and Haberland, Matt and Reddy, Tyler and Cournapeau, David and Burovski, Evgeni and Peterson, Pearu and Weckesser, Warren and Bright, Jonathan and

    Virtanen, Pauli and Gommers, Ralf and Oliphant, Travis E. and Haberland, Matt and Reddy, Tyler and Cournapeau, David and Burovski, Evgeni and Peterson, Pearu and Weckesser, Warren and Bright, Jonathan and. Nature Methods , year =

  10. [18]

    Journal of Power Sources , volume=

    The structure, composition, and performance impact of a YSZ-GDC interdiffusion layer in solid oxide electrolysis cells , author=. Journal of Power Sources , volume=. 2026 , publisher=

    2026

  11. [19]

    Journal of Power Sources , volume =

    Robust dynamic operation of high temperature electrolysis solid oxide cells , author =. Journal of Power Sources , volume =. 2026 , doi =

    2026

  12. [20]

    Zur theorie der spezifischen w

    Debye, Peter , journal=. Zur theorie der spezifischen w. 1912 , publisher=

    1912

  13. [21]

    Acta Materialia , volume=

    Control of grain growth using intergranular silicate phases in cubic yttria stabilized zirconia , author=. Acta Materialia , volume=. 1998 , publisher=

    1998

  14. [22]

    Synchrotron Radiation , volume=

    In situ observation of phase changes of a silica-supported cobalt catalyst for the Fischer--Tropsch process by the development of a synchrotron-compatible in situ/operando powder X-ray diffraction cell , author=. Synchrotron Radiation , volume=. 2018 , publisher=

    2018

  15. [23]

    Journal of Applied Physics , volume=

    Direct measurement of grain boundary enthalpy of cubic yttria-stabilized zirconia by differential scanning calorimetry , author=. Journal of Applied Physics , volume=. 2012 , publisher=

    2012

  16. [24]

    Acta materialia , volume=

    Grain-boundary structure and microstructure development mechanism in 2--8 mol\ author=. Acta materialia , volume=. 2008 , publisher=

    2008

  17. [25]

    Ceramics International , volume=

    EBSD analysis of microstructure changes in YSZ coatings during thermal cycling , author=. Ceramics International , volume=. 2021 , publisher=

    2021

  18. [26]

    Influence of the Rare Earth Cation on the Magnetic Properties of Layered 12R-Ba _4M^

    Dzara, Michael J and Campello, Arthur C and Breidenbach, Aeryn T and Strange, Nicholas A and Park, James Eujin and Ambrosini, Andrea and Coker, Eric N and Ginley, David S and Lee, Young S and Bell, Robert T and Rebecca W Smaha , journal=. Influence of the Rare Earth Cation on ...

    2024

  19. [27]

    , number =

    Coelho, Alan A. , number =. 2018 , journal =. doi:10.1107/S1600576718000183/HTTPS://JOURNALS.IUCR.ORG/SERVICES/RSS.HTML , issn =

    2018 doi

  20. [28]

    Frontiers in Physics , volume=

    A brief review of spin glass magnetometry techniques , author=. Frontiers in Physics , volume=. 2024 , publisher=

    2024

  21. [29]

    Jahn-Teller effect in the 4T _

    Manson, N B and Hasan, Z and Flint, C D , journal=. Jahn-Teller effect in the 4T _. 1979 , publisher=

    1979

  22. [30]

    Chemical Reviews , volume=

    Jahn--Teller and Pseudo-Jahn--Teller effects: from particular features to general tools in exploring molecular and solid state properties , author=. Chemical Reviews , volume=. 2020 , publisher=

    2020

  23. [31]

    Applied Crystallography , volume=

    Huq, Ashfia and Kirkham, Melanie and Peterson, Peter F and Hodges, Jason P and Whitfield, Pamela S and Page, Katharine and H. Applied Crystallography , volume=. 2019 , publisher=

    2019

  24. [32]

    Baur, W. H. , number =. 1974 , journal =. doi:10.1107/S0567740874004560 , issn =

    1974 doi

  25. [33]

    and Dutton, Siân E

    Nagle-Cocco, Liam A.V. and Dutton, Siân E. , number =. 2024 , journal =. doi:10.1107/S1600576723009925/HTTPS://JOURNALS.IUCR.ORG/SERVICES/RSS.HTML , issn =

    2024 doi

  26. [34]

    Foundations of Crystallography , volume=

    Tables of crystallographic properties of magnetic space groups , author=. Foundations of Crystallography , volume=. 2008 , publisher=

    2008

  27. [35]

    The Canadian Mineralogist , volume=

    Polyhedral volume calculations , author=. The Canadian Mineralogist , volume=. 1980 , publisher=

    1980

  28. [36]

    Van Vleck, J. H. , number =. 1939 , journal =. doi:10.1063/1.1750327 , issn =

    1939 doi

  29. [37]

    and Alexiu, Alexandra and Phillips, George S

    Genreith-Schriever, Annalena R. and Alexiu, Alexandra and Phillips, George S. and Coates, Chloe S. and Nagle-Cocco, Liam A. V. and Bocarsly, Joshua D. and Sayed, Farheen N. and Dutton, Siân E. and Grey, Clare P. , number =. 2024 , journal =. doi:10.1021/ACS.CHEMMATER.3C02413/SUPPL

    2024 doi

  30. [38]

    Journal of the American Chemical Society , volume=

    Regulating pseudo-Jahn--Teller effect and superstructure in layered cathode materials for reversible alkali-ion intercalation , author=. Journal of the American Chemical Society , volume=. 2022 , publisher=

    2022

  31. [39]

    Nagle-Cocco, Liam A. V. and Genreith-Schriever, Annalena R. and Steele, James M. A. and Tacconis, Camilla and Bocarsly, Joshua D. and Mathon, Olivier and Neuefeind, Joerg C. and Liu, Jue and O’Keefe, Christopher A. and Goodwin, Andrew L. and Grey, Clare P. and Evans, John S. O...

    2024 doi

  32. [40]

    Communications Physics , volume=

    Tutorial: a beginner’s guide to interpreting magnetic susceptibility data with the Curie-Weiss law , author=. Communications Physics , volume=. 2022 , publisher=

    2022

  33. [41]

    Inorganic Chemistry , volume=

    Crystal Growth, Structure, and Diverse Magnetic Behaviors in Frustrated Triangular Lattice REBO _3 (RE= Tb--Yb) , author=. Inorganic Chemistry , volume=. 2024 , publisher=

    2024

  34. [42]

    Zeitschrift f

    Crystal structure and specific heat of calcium lanthanide oxyborates Ca _4 LnO(BO _3 ) _3 , author=. Zeitschrift f. 2022 , publisher=

    2022

  35. [43]

    Materials Research Bulletin , volume=

    Magnetic properties of monoclinic lanthanide orthoborates, LnBO _3 , Ln= Gd, Tb, Dy, Ho, Er, Yb , author=. Materials Research Bulletin , volume=. 2018 , publisher=

    2018

  36. [44]

    Enhanced magnetocaloric effect from Cr substitution in Ising lanthanide gallium garnets Ln _3 CrGa _4 O _

    Mukherjee, Paromita and Dutton, Si. Enhanced magnetocaloric effect from Cr substitution in Ising lanthanide gallium garnets Ln _3 CrGa _4 O _. Advanced Functional Materials , volume=. 2017 , publisher=

    2017

  37. [45]

    Ground state of the easy-axis rare-earth kagome langasite Pr _3 Ga _5 SiO _

    Zorko, Andrej and Bert, Fabrice and Mendels, Philippe and Marty, Karol and Bordet, Pierre , journal=. Ground state of the easy-axis rare-earth kagome langasite Pr _3 Ga _5 SiO _. 2010 , publisher=

    2010

  38. [46]

    Journal of Physics: Condensed Matter , volume=

    Magnetic properties of monoclinic lanthanide metaborates, Ln(BO _2 ) _3 , Ln= Pr, Nd, Gd, Tb , author=. Journal of Physics: Condensed Matter , volume=. 2017 , publisher=

    2017

  39. [47]

    Inorganic Chemistry , volume=

    Magnetic properties of quasi-one-dimensional lanthanide calcium oxyborates Ca _4 LnO(BO _3 ) _3 , author=. Inorganic Chemistry , volume=. 2020 , publisher=

    2020

  40. [48]

    Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment , volume=

    A general purpose sub-keV X-ray facility at the Stanford Synchrotron Radiation Laboratory , author=. Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment , volume=. 1990 , publisher=

    1990

  41. [49]

    Beam line 2‑2 – general x‑ray absorption spectroscopy , howpublished =

  42. [50]

    Beam line 8‑2 – soft x‑ray absorption and photoemission spectroscopy , howpublished =

  43. [51]

    2018 , type =

    Sapana Tripathi , title =. 2018 , type =

    2018

  44. [52]

    Materials Research Bulletin , volume=

    Low temperature synthesis of LnOF rare-earth oxyfluorides through reaction of the oxides with PTFE , author=. Materials Research Bulletin , volume=. 2012 , publisher=

    2012

  45. [53]

    2005 , publisher=

    Ravel, B and Newville, M , journal=. 2005 , publisher=

    2005

  46. [54]

    2005 , publisher=

    Ravel, Bruce and Newville, M , journal=. 2005 , publisher=

    2005

  47. [55]

    2025 , journal =

    Steele, James M A and Genreith-Schriever, Annalena R and Bocarsly, Joshua D and Nagle-Cocco, Liam A V and Sayed, Farheen N and Juramy, Marie and O'Keefe, Christopher A and Orlandi, Fabio and Manuel, Pascal and Dutton, E S and Grey, Clare P , url =. 2025 , journal =

    2025

  48. [56]

    Khan, Safe and Aw, Eva S. Y. and Nagle-Cocco, Liam A. V. and Sud, Aakanksha and Ghosh, Sukanya and Subhan, Mohammed K.B. and Xue, Zekun and Freeman, Charlie and Sagkovits, Dimitrios and Guti. 2024 , journal =. doi:10.1002/ADMA.202400270 , issn =

    2024 doi

  49. [57]

    and Kelly, Nicola D

    Koskelo, Elise Anne C. and Kelly, Nicola D. and Nagle-Cocco, Liam A.V. and Bocarsly, Joshua D. and Mukherjee, Paromita and Liu, Cheng and Zhang, Qiang and Dutton, Siân E. , number =. 2023 , journal =. doi:10.1021/ACS.INORGCHEM.3C01137/ASSET/IMAGES/LARGE/IC3C01137

    2023 doi

  50. [58]

    R and Greedan, J

    Reimers, J N and Dahn, J. R and Greedan, J. E. and Stager, C. V. and Liu, G. and Davidson, I. and von Sacken, U. , number =. 1993 , journal =

    1993

  51. [59]

    1994 , journal =

    Suib, Steven L and Iton, Lennox E , pages =. 1994 , journal =

    1994

  52. [60]

    and Kong, Tai and Cava, R

    Nguyen, Loi T. and Kong, Tai and Cava, R. J. , number =. 2019 , journal =. doi:10.1088/2053-1591/ab0695 , issn =

    2019 doi

  53. [61]

    and Tang, Y

    Yang, H. and Tang, Y. K. and Yao, L. D. and Zhang, W. and Li, Q. A. and Li, F. Y. and Jin, C. Q. and Yu, R. C. , number =. 2007 , journal =. doi:10.1016/j.jallcom.2006.05.117 , issn =

    2007 doi

  54. [62]

    and Boulahya, Khalid and Amador, Ulises , number =

    Fuentes, Antonio F. and Boulahya, Khalid and Amador, Ulises , number =. 2004 , journal =. doi:10.1016/j.jssc.2003.08.025 , issn =

    2004 doi

  55. [63]

    and Cao, Z

    Yang, H. and Cao, Z. E. and Shen, X. and Feng, W. J. and Jiang, J. L. and Dai, J. F. and Yu, R. C. , number =. 2008 , journal =. doi:10.1007/s10853-008-2798-4 , issn =

    2008 doi

  56. [64]

    and Yang, Xiaohao and Billinge, Simon J.L

    Frandsen, Benjamin A. and Yang, Xiaohao and Billinge, Simon J.L. , number =. 2014 , journal =. doi:10.1107/S2053273313033081 , issn =

    2014 doi

  57. [65]

    and Hamilton, Parker K

    Baral, Raju and Christensen, Jacob A. and Hamilton, Parker K. and Ye, Feng and Chesnel, Karine and Sparks, Taylor D. and Ward, Rosa and Yan, Jiaqiang and McGuire, Michael A. and Manley, Michael E. and Staunton, Julie B. and Hermann, Raphaël P. and Frandsen, Benjamin A. , numbe...

    2022 doi

  58. [66]

    and Frandsen, Benjamin A

    Andersen, Henrik L. and Frandsen, Benjamin A. and Gunnlaugsson, Haraldur P. and J. 2021 , journal =. doi:10.1107/S2052252520013585 , issn =

    2021 doi

  59. [67]

    and Schulz, L

    Nuccio, L. and Schulz, L. and Drew, A. J. , number =. 2014 , booktitle =. doi:10.1088/0022-3727/47/47/473001 , issn =

    2014 doi

  60. [68]

    and Bell, Robert T

    Strange, Nicholas A. and Bell, Robert T. and Park, James Eujin and Stone, Kevin H. and Coker, Eric N. and Ginley, David S. , number =. 2023 , journal =. doi:10.1107/S2056989023003213/WM5677SUP3.TXT , issn =

    2023 doi

  61. [69]

    Streltsov, S. V. and Khomskii, D. I. , number =. 2018 , journal =. doi:10.1134/S0021364018220071 , issn =

    2018 doi

  62. [70]

    2015 , journal =

    Mac. 2015 , journal =. doi:10.1039/c4nj00798k , issn =

    2015 doi

  63. [71]

    Nagle-Cocco, Liam A. V. , title =. 2023 , url =

    2023

  64. [72]

    and Hayward, Michael A

    Adkin, Josephine J. and Hayward, Michael A. , number =. 2006 , journal =. doi:10.1016/j.jssc.2005.09.046 , issn =

    2006 doi

  65. [73]

    Debora and Sanders, Michael D

    Barcellos, R. Debora and Sanders, Michael D. and Tong, Jianhua and McDaniel, Anthony H. and O'Hayre, Ryan P. , number =. 2018 , journal =. doi:10.1039/c8ee01989d , issn =

    2018 doi

  66. [74]

    and Park, James Eujin and Goyal, Anuj and Bell, Robert T

    Strange, Nicholas A. and Park, James Eujin and Goyal, Anuj and Bell, Robert T. and Trindell, Jamie A. and Sugar, Joshua D. and Stone, Kevin H. and Coker, Eric N. and Lany, Stephan and Shulda, Sarah and Ginley, David S. , number =. 2022 , journal =. doi:10.1021/ACS.INORGCHEM.2C...

    2022 doi

  67. [75]

    and Sainio, Sami and Strange, Nicholas A

    Roychoudhury, Subhayan and Shulda, Sarah and Goyal, Anuj and Bell, Robert T. and Sainio, Sami and Strange, Nicholas A. and Park, James Eujin and Coker, Eric N. and Lany, Stephan and Ginley, David S. and Prendergast, David , number =. 2023 , journal =. doi:10.1021/acs.chemmater...

    2023 doi

  68. [76]

    2018 , journal =

    Tan, Zhenhong and Saito, Takashi and Denis Romero, Fabio and Amano Patino, Midori and Goto, Masato and Chen, Wei Tin and Chuang, Yu Chun and Sheu, Hwo Shuenn and Shimakawa, Yuichi , number =. 2018 , journal =. doi:10.1021/acs.inorgchem.8b01618 , issn =

    2018 doi

  69. [77]

    and Smith, Mark D

    Ferreira, Timothy and Heald, Steve M. and Smith, Mark D. and Zur Loye, Hans Conrad , number =. 2018 , journal =. doi:10.1021/acs.inorgchem.8b00249 , issn =

    2018 doi

  70. [78]

    2009 , journal =

    Shimoda, Yuki and Doi, Yoshihiro and Wakeshima, Makoto and Hinatsu, Yukio , number =. 2009 , journal =. doi:10.1021/ic9009652 , issn =

    2009 doi

  71. [79]

    2010 , journal =

    Shimoda, Yuki and Doi, Yoshihiro and Wakeshima, Makoto and Hinatsu, Yukio , number =. 2010 , journal =. doi:10.1016/j.jssc.2010.06.023 , issn =

    2010 doi

  72. [80]

    and Huang, Zixin and Mohamed, Zakiah and Kennedy, Brendan J

    Miiller, Wojciech and Dunstan, Matthew T. and Huang, Zixin and Mohamed, Zakiah and Kennedy, Brendan J. and Avdeev, Maxim and Ling, Chris D. , number =. 2013 , journal =. doi:10.1021/ic4014619 , issn =

    2013 doi

  73. [81]

    2008 , journal =

    Shimoda, Yuki and Doi, Yoshihiro and Hinatsu, Yukio and Ohoyama, Kenji , number =. 2008 , journal =. doi:10.1021/cm800708g , issn =

    2008 doi

  74. [82]

    2009 , journal =

    Shimoda, Yuki and Doi, Yoshihiro and Wakeshima, Makoto and Hinatsu, Yukio , number =. 2009 , journal =. doi:10.1016/j.jssc.2009.07.056 , issn =

    2009 doi

  75. [83]

    2023 , journal =

    Yan, Xiaohui and Wu, Junkun and Lei, Xiuyun and He, Lunhua and Guo, Wenbin and Kuang, Xiaojun and Yin, Congling , number =. 2023 , journal =. doi:10.1039/d3ra00607g , issn =

    2023 doi

  76. [84]

    2024 , journal =

    Ali, Anzar and Kim, Heung Sik and Yadav, Poonam and Lee, Suheon and Yoon, Duhee and Choi, Sungkyun , number =. 2024 , journal =. doi:10.1103/PhysRevResearch.6.013231 , issn =

    2024 doi

  77. [85]

    and Hughes, Helen and Rosseinsky, Matthew J

    Kuang, Xiaojun and Bridges, Craig and Allix, Mathieu and Claridge, John B. and Hughes, Helen and Rosseinsky, Matthew J. , number =. 2006 , journal =. doi:10.1021/cm0612752 , issn =

    2006 doi

  78. [86]

    2003 , journal =

    Cr. 2003 , journal =. doi:10.1016/S1293-2558(02)00098-5 , issn =

    2003 doi

  79. [87]

    and Ramanathan, Arun and Rice, Natalie T

    Gompa, Thaige P. and Ramanathan, Arun and Rice, Natalie T. and La Pierre, Henry S. , number =. 2020 , journal =. doi:10.1039/d0dt01400a , issn =

    2020 doi

  80. [88]

    2021-07-21 , doi =

    XAFS spectrum of Neodymium oxide , author =. 2021-07-21 , doi =

    2021

  81. [89]

    Ceramics International , volume=

    Effect of oxygen non-stoichiometry and redox phenomena in La/Ba--Sr--Co--Fe--O-based perovskite systems and its heterostructure as applicable in Solid Oxide Cell (SOC) air electrode , author=. Ceramics International , volume=. 2022 , publisher=

    2022

  82. [90]

    ECS Transactions , volume=

    Changes in LSC and LSCF cathode crystallographic parameters measured by electrochemical in situ high-temperature XRD , author=. ECS Transactions , volume=. 2013 , publisher=

    2013

  83. [91]

    Impact of the electrospinning synthesis route on the structural and electrocatalytic features of the LSCF (La0. 6Sr0. 4Co0. 2Fe0. 8O3-- ) perovskite for application in solid oxide fuel cells , author=. Solid State Ionics , volume=. 2024 , publisher=

    2024

  84. [92]

    Enhanced electrochemical redox kinetics of La0. 6Sr0. 4Co0. 2Fe0. 8O3 in reversible solid oxide cells , author=. Electrochimica Acta , volume=. 2023 , publisher=

    2023

  85. [93]

    Local structure change around Co and Fe ions in (La0. 6Sr0. 4)(Co0. 2Fe0. 8) O3- as revealed by in--situ X--ray absorption spectroscopy and first--principles calculation , author=. Journal of Solid State Chemistry , volume=. 2018 , publisher=

    2018

  86. [94]

    Journal of Alloys and Compounds , volume=

    Electrochemical behavior of LSCF/GDC interface in symmetric cell: An application in solid oxide fuel cells , author=. Journal of Alloys and Compounds , volume=. 2015 , publisher=

    2015

  87. [95]

    Solid state sciences , volume=

    Physicochemical compatibility of CGO fluorite, LSM and LSCF perovskite electrode materials with La2Mo2O9 fast oxide-ion conductor , author=. Solid state sciences , volume=. 2005 , publisher=

    2005

  88. [96]

    Journal of Materials Chemistry A , volume=

    An efficient and robust lanthanum strontium cobalt ferrite catalyst as a bifunctional oxygen electrode for reversible solid oxide cells , author=. Journal of Materials Chemistry A , volume=. 2021 , publisher=

    2021

  89. [97]

    Applied Catalysis B: Environmental , volume=

    Concurrent promotion of phase transition and bimetallic nanocatalyst exsolution in perovskite oxides driven by Pd doping to achieve highly active bifunctional fuel electrodes for reversible solid oxide electrochemical cells , author=. Applied Catalysis B: Environmental , volum...

    2022

  90. [98]

    Mechanical aspects of ferro-elastic behavior and phase composition of La0. 58Sr0. 4Co0. 2Fe0. 8O3- , author=. Journal of membrane science , volume=. 2010 , publisher=

    2010

  91. [99]

    Solid State Ionics , volume=

    Direct observation of ferroelastic domain effects in LSCF perovskites , author=. Solid State Ionics , volume=. 2012 , publisher=

    2012

  92. [100]

    Bulletin of Materials Science , volume=

    Effect of processing route on the properties of LSCF-based composite cathode for IT-SOFC , author=. Bulletin of Materials Science , volume=. 2020 , publisher=

    2020

  93. [101]

    ACS Physical Chemistry Au , volume=

    Understanding (La, Sr)(Co, Fe) O3- Phase Instability within SOECs Using a Combined Experimental and Atomistic Modeling Approach , author=. ACS Physical Chemistry Au , volume=. 2025 , publisher=

    2025

  94. [102]

    Ceramics International , volume=

    Rietveld refinement and estimation of residual stress in GDC--LSCF oxygen transport membrane ceramic composites , author=. Ceramics International , volume=. 2018 , publisher=

    2018

  95. [103]

    Crystal Research and Technology , volume=

    Synthesis, structure and electrochemical performance of cobaltite-based composite cathodes for IT-SOFC , author=. Crystal Research and Technology , volume=. 2012 , publisher=

    2012

  96. [104]

    Journal of power sources , volume=

    Lattice expansion of LSCF-6428 cathodes measured by in situ XRD during SOFC operation , author=. Journal of power sources , volume=. 2012 , publisher=

    2012

  97. [105]

    Crystal structure, cobalt and iron speciation and oxygen non-stoichiometry of La0. 6Sr0. 4Co1-yFeyO3- nanorods for IT-SOFC cathodes , author=. Journal of Alloys and Compounds , volume=. 2020 , publisher=

    2020

  98. [106]

    Rietveld, H. M. , number =. 1969 , journal =. doi:10.1107/S0021889869006558 , issn =

    1969 doi

  99. [107]

    Patterson, A. L. , number =. 1939 , journal =. doi:10.1103/PhysRev.56.978 , issn =

    1939 doi

  100. [108]

    and Ozkan, Umit S

    Kuhn, John N. and Ozkan, Umit S. , number =. 2008 , journal =. doi:10.1007/s10562-007-9364-6 , issn =

    2008 doi

  101. [109]

    2012 , journal =

    Itoh, Takanori and Nakayama, Masanobu , volume =. 2012 , journal =. doi:10.1016/j.jssc.2012.03.021 , issn =

    2012 doi

  102. [110]

    and Lane, J

    Waller, D. and Lane, J. A. and Kilner, J. A. and Steele, B. C.H. , number =. 1996 , journal =. doi:10.1016/0167-2738(96)00362-1 , issn =

    1996 doi

  103. [111]

    2022 , journal =

    Cai, Changkun and Xie, Manyi and Xue, Ke and Shi, Yu and Li, Shuting and Liu, Yuanyuan and An, Shengli and Yang, Hong , number =. 2022 , journal =. doi:10.1007/s12274-021-3972-0 , issn =

    2022 doi

  104. [112]

    and Lane, J

    Waller, D. and Lane, J. A. and Kilner, J. A. and Steele, B. C.H. , number =. 1996 , journal =. doi:10.1016/0167-577X(95)00289-8 , issn =

    1996 doi

  105. [113]

    and Williams, Robert and Kemen, Nils and McComb, David W

    Ni, Na and Cooper, Samuel J. and Williams, Robert and Kemen, Nils and McComb, David W. and Skinner, Stephen J. , number =. 2016 , journal =. doi:10.1021/acsami.6b05290 , issn =

    2016 doi

  106. [114]

    2018 , journal =

    Zou, Ying and Ziegner, Mirko and Malzbender, Jürgen and Kr. 2018 , journal =. doi:10.1016/j.ceramint.2017.11.026 , issn =

    2018 doi

  107. [115]

    Open Ceramics , pages=

    Formulation-driven additive manufacturing of 3YSZ advanced ceramics via digital light processing , author=. Open Ceramics , pages=. 2025 , publisher=

    2025

  108. [116]

    Ceramics International , volume=

    Structure, microstructure and electrical conductivity of 8YSZ containing NiO , author=. Ceramics International , volume=. 2011 , publisher=

    2011

  109. [117]

    High-temperature thermal cycling effect on the irreversible responses of lattice structure, magnetic properties, and electrical conductivity in Co2. 75Fe0. 25O4+ spinel oxide , author=. Inorganic Chemistry , volume=. 2020 , publisher=

    2020

  110. [118]

    Journal of Solid State Chemistry , volume=

    On the crystallographic and magnetic structures of nearly stoichiometric iron monoxide , author=. Journal of Solid State Chemistry , volume=. 1996 , publisher=

    1996

  111. [119]

    Journal of Applied Crystallography , year =

    Rietveld refinement of Debye--Scherrer synchrotron X-ray data from Al _2 O _3 , author =. Journal of Applied Crystallography , year =

  112. [120]

    Structural Science , volume=

    The structure of magnetite , author=. Structural Science , volume=. 1981 , publisher=

    1981

  113. [121]

    Structural Science , volume=

    The structure of cobalt oxide, Co _3 O _4 , author=. Structural Science , volume=. 1973 , publisher=

    1973

  114. [122]

    Applied Crystallography , volume=

    Unit-cell refinement from powder diffraction scans , author=. Applied Crystallography , volume=. 1981 , publisher=

    1981

  115. [123]

    Hunter, J. D. , Title =. Computing in Science & Engineering , Volume =

  116. [124]

    Applied Crystallography , volume=

    A profile refinement method for nuclear and magnetic structures , author=. Applied Crystallography , volume=. 1969 , publisher=

    1969

  117. [125]

    1995 , publisher=

    Python reference manual , author=. 1995 , publisher=

    1995

  118. [126]

    American Mineralogist , volume=

    Deciphering Ni sequestration in soil ferromanganese nodules by combining X-ray fluorescence, absorption, and diffraction at micrometer scales of resolution , author=. American Mineralogist , volume=. 2002 , publisher=

    2002

  119. [127]

    Journal of the American Chemical Society , volume=

    X-ray diffraction studies of systems involved in the preparation of alkaline earth sulfide and selenide phosphors1 , author=. Journal of the American Chemical Society , volume=. 1948 , publisher=

    1948

  120. [128]

    Synthesis, structural characterization, and studies of magnetic and dielectric properties of Gd ^

    Bandyopadhyay, A and Sarkar, B J and Sutradhar, S and Mandal, J and Chakrabarti, P K , journal=. Synthesis, structural characterization, and studies of magnetic and dielectric properties of Gd ^. 2021 , publisher=

    2021

  121. [129]

    Journal of the American Ceramic Society , volume=

    Solid Solubility and Lattice Parameter of NiO-MnO , author=. Journal of the American Ceramic Society , volume=. 1964 , publisher=

    1964

  122. [130]

    Physical Review , volume=

    X-ray crystal analysis of thirteen common metals , author=. Physical Review , volume=. 1921 , publisher=

    1921

  123. [131]

    Canadian Journal of Earth Sciences , volume=

    Micro X-ray diffraction ( XRD): a versatile technique for characterization of Earth and planetary materials , author=. Canadian Journal of Earth Sciences , volume=. 2007 , publisher=

    2007

  124. [132]

    Chemistry--A European Journal , volume=

    X-ray diffraction mapping for cultural heritage science: a review of experimental configurations and applications , author=. Chemistry--A European Journal , volume=. 2020 , publisher=

    2020

  125. [133]

    Journal of analytical atomic spectrometry , volume=

    Applications of synchrotron-based micro-imaging techniques to the chemical analysis of ancient paintings , author=. Journal of analytical atomic spectrometry , volume=. 2008 , publisher=

    2008

  126. [134]

    Applied Crystallography , volume=

    XRDUA: crystalline phase distribution maps by two-dimensional scanning and tomographic (micro) X-ray powder diffraction , author=. Applied Crystallography , volume=. 2014 , publisher=

    2014

  127. [135]

    arXiv preprint arXiv:2403.10042 , year=

    Accurate and Data-Efficient Micro-XRD Phase Identification Using Multi-Task Learning: Application to Hydrothermal Fluids , author=. arXiv preprint arXiv:2403.10042 , year=

    arXiv

  128. [136]

    Applied Crystallography , volume=

    Nika: software for two-dimensional data reduction , author=. Applied Crystallography , volume=. 2012 , publisher=

    2012

  129. [137]

    Synchrotron Radiation , volume=

    An X-ray beamline for utilizing intense, high-energy undulator radiation , author=. Synchrotron Radiation , volume=. 2025 , publisher=

    2025

  130. [138]

    Synchrotron Radiation , volume=

    A micro-focusing and high-flux-throughput beamline design using a bending magnet for microscopic XAFS at the High Energy Photon Source , author=. Synchrotron Radiation , volume=. 2019 , publisher=

    2019

  131. [139]

    Synchrotron Radiation , volume=

    Focusing X-ray free-electron laser pulses using Kirkpatrick--Baez mirrors at the NCI hutch of the PAL-XFEL , author=. Synchrotron Radiation , volume=. 2018 , publisher=

    2018

  132. [140]

    Scientific Reports , volume=

    Anisotropic chemical expansion due to oxygen vacancies in perovskite films , author=. Scientific Reports , volume=. 2021 , publisher=

    2021

  133. [141]

    Kaufman, J. L. and Lei, Y. and Nagle-Cocco, L. A. V. and Kane, N. J. and Rowberg, A. J. E. and Hartvigsen, J. L. and Strange, N. A. and Abernathy, H. and Wood, B. C. and Kweon, K. E. , title =. In preparation , year=

  134. [142]

    Materials Letters , volume=

    Microstructure of a solid oxide fuel cell by microbeam X-ray diffraction , author=. Materials Letters , volume=. 2020 , publisher=

    2020

  135. [143]

    Scientific Reports , volume=

    Deep learning of structural morphology imaged by scanning X-ray diffraction microscopy , author=. Scientific Reports , volume=. 2025 , publisher=

    2025

  136. [144]

    Hong and M

    Y. Hong and M. D. Balcazar and R. Robles and R. Arthur and C. Takacs and T. Sato and D. Zhu and A. Halavanau , title =. Proceedings of the North American Particle Accelerator Conference (NAPAC2025) , year =. doi:10.18429/JACoW-NAPAC2025-THP027 , isbn =

    doi

  137. [145]

    Journal of power sources , volume=

    Microstructural comparison of solid oxide electrolyser cells operated for 6100 h and 9000 h , author=. Journal of power sources , volume=. 2015 , publisher=

    2015

  138. [146]

    Long-term degradation of La0. 6Sr0. 4Co0. 2Fe0. 8O3- IT-SOFC cathodes due to silicon poisoning , author=. Solid State Ionics , volume=. 2016 , publisher=

    2016

  139. [147]

    Chemistry of Materials , volume=

    Onset Reaction Mechanism of Cr and S Poisoning on Perovskite Oxide Surfaces , author=. Chemistry of Materials , volume=. 2024 , publisher=

    2024

  140. [148]

    Chemie Ingenieur Technik , volume=

    Microkinetic modeling of nickel oxidation in solid oxide cells: prediction of safe operating conditions , author=. Chemie Ingenieur Technik , volume=. 2019 , publisher=

    2019

  141. [149]

    Physical Chemistry Chemical Physics , volume=

    Chromium deposition and poisoning at La 0.6 Sr 0.4 Co 0.2 Fe 0.8 O 3- oxygen electrodes of solid oxide electrolysis cells , author=. Physical Chemistry Chemical Physics , volume=. 2015 , publisher=

    2015

  142. [150]

    Journal of The Electrochemical Society , volume=

    SrZrO3 formation at the interlayer/electrolyte interface during (La1-xSrx) 1- Co1-yFeyO3 cathode sintering , author=. Journal of The Electrochemical Society , volume=. 2017 , publisher=

    2017

  143. [151]

    Chemistry of Materials , volume=

    Impact of Sr-Containing Secondary Phases on Oxide Conductivity in Solid-Oxide Electrolyzer Cells , author=. Chemistry of Materials , volume=. 2024 , publisher=

    2024

  144. [152]

    Journal of Power Sources , volume=

    Voltage cycling as a dynamic operation mode for high temperature electrolysis solid oxide cells , author=. Journal of Power Sources , volume=. 2025 , publisher=

    2025

  145. [153]

    Science , volume=

    Recent advances in solid oxide cell technology for electrolysis , author=. Science , volume=. 2020 , publisher=

    2020

  146. [154]

    and Kane, Nicholas and Hartvigsen, Jeremy L

    Crain, Christopher A. and Kane, Nicholas and Hartvigsen, Jeremy L. and Casteel, Micah and Arthur, Ross J. and Reynolds, Katerina and Tucker, Michael C. and Shulda, Sarah and Ginley, David S. and Strange, Nicholas A. , number =. 2026 , journal =. doi:10.1021/acs.chemmater.5c032...

    2026 doi

  147. [155]

    Nagle-Cocco, L. A. V. , title =. 2026 , publisher =

    2026

Pith tools

Reviewed August 3, 2026 · model on record in the stance chip above.