Pith. sign in

REVIEW

Not yet reviewed by Pith; the record is open.

This paper has not been read by Pith yet. Machine review is queued; the pith claim, tier, and objections will appear here once it completes.

SPECIMEN: schema-true, not a live event

T0 review · schema-true

One-sentence machine reading of the paper's core claim.

pith:XXXXXXXX · record.json · timestamp

arxiv cond-mat/0102498 v2 pith:PX6P37J6 submitted 2001-02-27 cond-mat.supr-con

Microstructure of the highly dense MgB2 Superconductor by transmission electron microscope

classification cond-mat.supr-con
keywords highmgb2electrongrainhrteminvestigatedmicroscopemicrostructure
verification ladder T0 review T1 audit T2 compute T3 formal T4 reserved
0 comments
read the original abstract

The microstructure of the MgB2 superconductor sintered at high temperature under a high pressure of about 3 GPa was investigated by using a high-resolution transmission electron microscope (HRTEM). The TEM images did not show any pores in the specimen. All grains were compactly connected, and no discernable empty spaces or impurities at the boundaries existed over the regions investigated. The HRTEM image showed clearly each constituent atom that formed the basal hexagonal plane, without any defect in a single grain. The a-axis lattice parameter, 0.307 nm, from this direct measurement was shorter than the value, 0.314 nm obtained from samples prepared using diffusion techniques. A minor impurity phase, which was most probably MgB4 and did not form interfacial layers was also observed, but was well isolated from the main MgB2 phase. Our results verify that the MgB2 powder was sintered under high temperature and high pressure into its theoretical density without any porosity or grain growth.

discussion (0)

Sign in with ORCID, Apple, or X to comment. Anyone can read and Pith papers without signing in.